Technical Brief

The Effect of Cryogenic Treatment on Microstructure and Mechanical Response of AISI D3 Tool Steel Punches

[+] Author and Article Information
Y. Arslan

Duzce University,
Duzce Vocational High School,
Uzunmustafa Mahallesi Duzce 81100, Turkey
e-mail: yusufarslan@duzce.edu.tr

I. Uygur

Department of Mechanical Engineering,
Faculty of Engineering,
Duzce University,
Konuralp Campus,
Duzce 81620, Turkey
e-mail: ilyasuygur@duzce.edu.tr

A. Jazdzewska

Department of Electrochemistry,
Corrosion and Materials Engineering,
Gdansk University of Technology, 11/12,
Gdansk 80-233, Poland
e-mail: paquitaxp@gmail.com

1Corresponding author.

Contributed by the Manufacturing Engineering Division of ASME for publication in the JOURNAL OF MANUFACTURING SCIENCE AND ENGINEERING. Manuscript received July 21, 2014; final manuscript received December 24, 2014; published online February 16, 2015. Assoc. Editor: Gracious Ngaile.

J. Manuf. Sci. Eng 137(3), 034501 (Jun 01, 2015) (6 pages) Paper No: MANU-14-1403; doi: 10.1115/1.4029567 History: Received July 21, 2014; Revised December 24, 2014; Online February 16, 2015

Recently, deep cryogenic treatment is performed to improve the mechanical responses (wear, hardness, fatigue, and thermal conductivity) of various steel components. Researchers have tried to evaluate the eco-friendly and nontoxic process to optimize the parameters. Cold-shearing punches used to manufacture various holes that undergo severe impact loading and wear in the metal forming process. This study concerns the effect of soaking time (24 hr, 36 hr) at liquid nitrogen temperature (−145 °C) during the deep cryogenic treatment on the microstructural changes which are carbide distribution and retained austenite percentage of AISI D3 tool steel punches. It was shown that the deep cryogenic treatment reduces retained austenite and enhanced uniform distribution of carbide particles. It is concluded that for significantly improved punch life and performance, it is an advisable application of 36 hr deep cryogenic treatment.

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Brownlee, K. G., and Smythe, T. W., 1970, “Punchability of Fully Processed Electrical Steel Sheet,” J. Iron Steel Inst., 208, pp. 806–812.
Wessel, J. K., 2004, Handbook of Advanced Materials: Enabling New Designs, Wiley-Interscience, Oak Ridge, TN.
Tapia, G., and Elwany, A., 2014, “A Review on Process Monitoring and Control in Metal-Based Additive Manufacturing,” ASME J. Manuf. Sci. Eng., 136(6), p. 060801. [CrossRef]
Hossain, M. S., Espalin, D., Ramos, J., Perez, M., and Wicker, R., 2014, “Improved Mechanical Properties of Fused Deposition Modeling-Manufactured Parts Through Build Parameter Modifications,” ASME J. Manuf. Sci. Eng., 136(6), p. 061002. [CrossRef]
Haapala, K. R., Zhao, F., Camelio, J., Sutherland, J. W., Skerlos, S. J., Dornfeld, D. A., Jawahir, I. S., Clarens, A. F., and Rickli, J. M., 2013, “A Review of Engineering Research in Sustainable Manufacturing,” ASME J. Manuf. Sci. Eng., 135(4), p. 041013. [CrossRef]
Attanasio, A., Ceretti, E., Giardini, C., and Cappellini, C., 2013, “Tool Wear in Cutting Operations: Experimental Analysis and Analytical Models,” ASME J. Manuf. Sci. Eng., 135(5), p. 051012. [CrossRef]
Park, K.-H., Beal, A., Kim, D., Kwon, P., and Lantrip, J., 2013, “A Comparative Study of Carbide Tools in Drilling of CFRP and CFRP-Ti Stacks,” ASME J. Manuf. Sci. Eng., 136(1), p. 014501. [CrossRef]
Hosseini, A., and Kishawy, H. A., 2013, “On the Optimized Design of Broaching Tools,” ASME J. Manuf. Sci. Eng., 136(1), p. 011011. [CrossRef]
Fehrenbacher, A., Schmale, J. R., Zinn, M. R., and Pfefferkorn, F. E., 2014, “Measurement of Tool-Workpiece Interface Temperature Distribution in Friction Stir Welding,” ASME J. Manuf. Sci. Eng., 136(2), p. 021009. [CrossRef]
dos Santos, R. G., and Coelho, R. T., 2014, “A Contribution to Improve the Accuracy of Chatter Prediction in Machine Tools Using the Stability Lobe Diagram,” ASME J. Manuf. Sci. Eng., 136(2), p. 021005. [CrossRef]
Braglia, M., and Castellano, D., 2014, “Diffusion Theory Applied to Tool-Life Stochastic Modeling Under a Progressive Wear Process,” ASME J. Manuf. Sci. Eng., 136(3), p. 031010. [CrossRef]
Pan, Y., Zhou, C., Chen, Y., and Partanen, J., 2014, “Multitool and Multi-Axis Computer Numerically Controlled Accumulation for Fabricating Conformal Features on Curved Surfaces,” ASME J. Manuf. Sci. Eng., 136(3), p. 031007. [CrossRef]
Wang, X., and Kwon, P. Y., 2014, “WC/Co Tool Wear in Dry Turning of Commercially Pure Aluminium,” ASME J. Manuf. Sci. Eng., 136(3), p. 031006. [CrossRef]
Pérez, R., Molina, A., and Ramírez-Cadena, M., 2014, “Development of an Integrated Approach to the Design of Reconfigurable Micro/Mesoscale CNC Machine Tools,” ASME J. Manuf. Sci. Eng., 136(3), p. 031003. [CrossRef]
Au, K. M., and Yu, K. M., 2014, “Variable Distance Adjustment for Conformal Cooling Channel Design in Rapid Tool,” ASME J. Manuf. Sci. Eng., 136(4), p. 044501. [CrossRef]
Li, Z.-L., and Zhu, L.-M., 2014, “Envelope Surface Modeling and Tool Path Optimization for Five-Axis Flank Milling Considering Cutter Runout,” ASME J. Manuf. Sci. Eng., 136(4), p. 041021. [CrossRef]
Mohan, L. D., Renganarayanan, S., and Kalanidhi, A., 2001, “Cryogenic Treatment to Augment Wear Resistance of Tool and Die Steels,” Cryogenics, 41(3), pp. 149–155. [CrossRef]
Singh, J., Singh, L. P., and Kaushik, A., 2013, “Enhancing Wear Resistance of En45 Spring Steel Using Cryogenic Treatment,” Frict. Wear Res., 1, pp. 22–27.
Jerold, B. D., and Kumar, M. P., 2013, “The Influence of Cryogenic Coolants in Machining of Ti–6Al–4V,” ASME J. Manuf. Sci. Eng., 135(3), p. 031005. [CrossRef]
Çiçek, A., Uygur, I., Kıvak, T., and Ozbek, N. A., 2012, “Machinability of AISI 316 Austenitic Stainless Steel With Cryogenically Treated M35 High-Speed Steel Twist Drills,” ASME J. Manuf. Sci. Eng., 134(6), p. 061003. [CrossRef]
Collins, D. N., 1996, “Deep Cryogenic Treatment of Tool Steels: A Review,” Heat Treat. Met., 2, pp. 40–42.
Firouzdor, V., Nejati, E., and Khomamizadeh, F., 2008, “Effect of Deep Cryogenic Treatment on Wear Resistance and Tool Life of M2 HSS Drill,” J. Mater. Process. Technol., 206(1–3), pp. 467–472. [CrossRef]
Blankinship, S., 2001, “Ultra-Cold Could Help Freeze Plant Repairs,” Power Eng., 105, pp. 13–16.
Gill, S. S., Singh, J., Singh, R., and Singh, H., 2011, “Metallurgical Principles of Cryogenically Treated Tool Steels-a Review on the Current State of Science,” Int. J. Adv. Manuf. Technol., 54(1–4), pp. 59–82. [CrossRef]
Siller, H. R., Vila, C., Rodriguez, A., and Abelan, J. V., 2009, “Study of Face Milling of Hardened AISI D3 Steel With a Special Design of Carbide Tools,” Int. J. Adv. Manuf. Technol., 40(1–2), pp. 12–25. [CrossRef]
Aslan, E., 2005, “Experimental Investigation of Cutting Tool Performance in High Speed Cutting of Hardened X210 Cr 12 Cold Work Tool Steel,” Mater. Des., 26(1), pp. 21–27. [CrossRef]
Tamizharasan, T., Selvaraj, T., and Haq, A. N., 2006, “Analysis of Tool Wear and Surface Finish in Hard Turning,” Int. J. Adv. Manuf. Technol., 28(7–8), pp. 671–679. [CrossRef]
Çiçek, A., Kıvak, T., Uygur, I., Ekici, E., and Turgut, Y., 2012, “Performance of Cryogenically Treated M35 HSS Drills in Drilling of Austenic Stainless Steels,” Int. J. Adv. Manuf. Technol., 60(1–4), pp. 65–73. [CrossRef]
ASTM E975-00, 2005, “Standard Practice for X-Ray Determination of Retained Austenite in Steel With Near Random Crystallographic Orientation,” ASTM Book of Standards, V03.01, West Conshohocken, PA.
Collins, D. N., and Dormer, J., 1997, “Deep Cryogenic Treatment of a D2 Cold-Worked Tool Steel,” Heat Treat. Met., 24, pp. 71–74.
Das, D., Dutta, A. K., and Ray, K. K., 2010, “Sub-Zero Treatments of AISI D2 Steel: Part I. Microstructure and Hardness,” Mater. Sci. Eng., A, 527(9), pp. 2182–2193. [CrossRef]
Das, D., Dutta, A. K., and Ray, K. K., 2009, “Influence of Varied Cryotreatment on Wear Behaviour of AISI D2 Steel,” Wear, 266(1–2), pp. 297–309. [CrossRef]
Huang, J. Y., Zhu, Y. T., Liao, X. Z., Beyerlein, I. J., Bourke, M. A., and Mitchell, T. E., 2003, “Microstructure of Cryogenic Treated M2 Tool Steel,” Mater. Sci. Eng., A, 339(1–2), pp. 241–244. [CrossRef]
Luo, S. Y., 1999, “Effect of the Geometry and the Surface Treatment of Punching Tools on the Tool Life and Wear Conditions in the Piercing of Thick Steel Plate,” J. Mater. Process. Technol., 88(1–3), pp. 122–133. [CrossRef]
Myint, M. H., Fuh, J. Y. H., Wong, Y. S., Lu, L., Chen, Z. D., and Choy, C. M., 2003, “Evaluation of Wear Mechanisms of Y-TZP and Tungsten Carbide Punches,” J. Mater. Process. Technol., 140(1–3), pp. 460–464. [CrossRef]
Lee, Y. C., and Chen, F. K., 2000, “Failure Analysis of a Cold-Extrusion Punch to Enhance Its Quality and Prolong Its Life,” J. Mater. Process. Technol., 105(1–2), pp. 134–142. [CrossRef]


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Fig. 1

A Schematic presentation of the heat treatment schedule consisting of hardening, deep cryogenic treatment, and tempering cycles of the punches

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Fig. 2

Various diameters of punches and dies

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Fig. 3

SEM pictures: (a) HT, (b) 24 CT and typical EDX analysis of point 2 (c) and (d) 4 in HT specimen

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Fig. 4

X-ray Diffraction line profiles (a) HT and (b) 36 CT specimens. The set of (hkl) in vertical direction indicates the 2θ positions of different diffraction planes of martensite, austenite, ferrite, Cr23 C6, Cr7C3, Fe3C, Fe7C, and M7C3 carbides.

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Fig. 5

Variation of (a) top surface wear and (b) flank wear of the punches (5 mm diameter) made of AISI D3 tool steels

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Fig. 6

Top surface of the HT punch made of D3, before and after trial blank process

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Fig. 7

Flank surface wear of punches after trial blank process. (a) 6000 strokes and (b) 40.000 strokes.

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Fig. 8

SEM micrograph of the top and flank surface (a) HT and (b) 36 CTT punches




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